Desenvolvimento de camadas ricas no intermetálico α-Alx(Fe,Mn,Cr)ySiz em ligas Al-Si por solidificação controlada
The intermetallic with high mechanical properties and good thermal stability can act as reinforcement in the aluminum matrix. This study evaluated the formation and properties of layers rich in intermetallic α-Alx(Fe,Mn,Cr)ySiz from the controlled solidification of multicomponent aluminum alloys. Th...
| Autor principal: | Ferreira, Tales |
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| Formato: | Dissertação |
| Idioma: | Português |
| Publicado em: |
Universidade Tecnológica Federal do Paraná
2017
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| Assuntos: | |
| Acesso em linha: |
http://repositorio.utfpr.edu.br/jspui/handle/1/1969 |
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| Resumo: |
The intermetallic with high mechanical properties and good thermal stability can act as reinforcement in the aluminum matrix. This study evaluated the formation and properties of layers rich in intermetallic α-Alx(Fe,Mn,Cr)ySiz from the controlled solidification of multicomponent aluminum alloys. Their primary formation takes place under specific chemical compositions and depends on the amount of Fe, the Mn/Fe ratio and cooling rate. In this work the melting and controlled solidification of aluminum alloy Al-Si-Cu-Fe-Mn, seeking the formation conditions of intermetallic α- Alx(Fe,Mn,Cr)ySiz. Analysis of differential scanning calorimetry (DSC) were performed this initial alloy. Based on BR102015013352-9 patent pending assembled into a solidification equipment controlled type "outward" pilot scale (10-15kg), coupled to a rotational matrix Fe-C (substrate) controlled peripheral speed. Solidified regions were evaluated by optical emission spectroscopy, XRD, optical microscopy and scanning/EDS. Mechanical properties were evaluated by hardness techniques Rockwell B (HRB) and Vickers hardness (HV). The open cell photoacoustic technique (OPC) was used for analyzing the thermal properties of the solidified samples. Regions having different mechanical properties and chemical compositions have been identified within the ingot. There was intense formation of the intermetallic compound α- Al15(Fe,Mn,Cr)4Si2 and, associated with this, severe chemical segregation in the regions adjacent to the substrate. HRB hardness variations were also observed in the different regions. The primary intermetallic α-Al15(Fe,Mn,Cr)4Si2 had a significant influence on thermal alloy aluminum Al-Si-Cu-Fe-Mn-Cr diffusivity. |
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